Reaktion #58512

ord-05f67a3f27674791aee08b5008da6f65

Reaktionsgleichung

CC(N)c1ccc([N+](=O)[O-])cc1
1-(4-nitro-phenyl)-ethylamine
COC(=O)c1ccc(C(=O)O)s1
thiophene-2,5-dicarboxylic acid monomethyl ester
→
COC(=O)c1ccc(C(=O)NC(C)c2ccc([N+](=O)[O-])cc2)s1
title compound
COC(=O)c1ccc(C(=O)NC(C)c2ccc([N+](=O)[O-])cc2)s1
5-[1-(4-Nitro-phenyl)-ethylcarbamoyl]-thiophene-2-carboxylic acid methyl ester

Edukte

CC(N)c1ccc([N+](=O)[O-])cc1
1-(4-nitro-phenyl)-ethylamine
COC(=O)c1ccc(C(=O)O)s1
thiophene-2,5-dicarboxylic acid monomethyl ester

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared in an analogous manner to that described in example 1, step 3 from 1-(4-nitro-phenyl)-ethylamine and thiophene-2,5-dicarboxylic acid monomethyl ester.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423060B2uspto-grants-2008_09