Reaktion #58312

Reaktionsgleichung

2-bromo-5-methoxybenzoic acid

n-butyllithium

N-methoxy-N-methylnicotinamide

→

5-methoxy-2-pyridin-3-ylbenzoic acid

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound is synthesized
2. 2
   SonstigeAfter precipitation in aqueous phase at pH 4
3. 3
   Filtrationfollowed by filtration
4. 4
   Sonstigedrying
5. 5
   Sonstigea beige-coloured powder is obtained

Vorschrift

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-N-methylnicotinamide. After precipitation in aqueous phase at pH 4, followed by filtration and drying, a beige-coloured powder is obtained.

Quelle