Reaktion #58250

ord-c65265230f564feb9a793b2bc6ea9eb5

Reaktionsgleichung

CCc1n[nH]c(=O)c2cc(OC)cc(OC)c12
5,7-dimethoxy-4-ethyl-2H-phthalazin-1-one
O=P(Cl)(Cl)Cl
phosphoryl chloride
→
CCc1nnc(Cl)c2cc(OC)cc(OC)c12
1-Chloro-5,7-dimethoxy-4-ethylphthalazine

Edukte

CCc1n[nH]c(=O)c2cc(OC)cc(OC)c12
5,7-dimethoxy-4-ethyl-2H-phthalazin-1-one
O=P(Cl)(Cl)Cl
phosphoryl chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound is obtained

Vorschrift

This compound is obtained according to the procedure described in 1.3. by reacting 5,7-dimethoxy-4-ethyl-2H-phthalazin-1-one with phosphoryl chloride.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423030B2uspto-grants-2008_09