Reaktion #58249

ord-8addd2b1950349888f92f8090aaddd30

Reaktionsgleichung

CCC(=O)c1c(OC)cc(OC)cc1C(=O)O
3,5-dimethoxy-2-propionylbenzoic acid
NN.O
hydrazine hydrate
→
CCc1n[nH]c(=O)c2cc(OC)cc(OC)c12
5,7-Dimethoxy-4-ethyl-2H-phthalazin-1-one

Edukte

CCC(=O)c1c(OC)cc(OC)cc1C(=O)O
3,5-dimethoxy-2-propionylbenzoic acid
NN.O
hydrazine hydrate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound is obtained

Vorschrift

This compound is obtained according to the procedure described in 1.2. by reacting unpurified 3,5-dimethoxy-2-propionylbenzoic acid with hydrazine hydrate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423030B2uspto-grants-2008_09