Reaktion #58245

ord-1587eedcedd5421b967eb8f1d3195542

Reaktionsgleichung

COc1cc(OC)c(C(=O)Cc2ccccc2)c(C(=O)O)c1
3,5-dimethoxy-2-(phenylacetyl)benzoic acid
NN.O
hydrazine hydrate
→
COc1cc(OC)c2c(Cc3ccccc3)n[nH]c(=O)c2c1
4-Benzyl-5,7-dimethoxy-2H-phthalazin-1-one

Edukte

COc1cc(OC)c(C(=O)Cc2ccccc2)c(C(=O)O)c1
3,5-dimethoxy-2-(phenylacetyl)benzoic acid
NN.O
hydrazine hydrate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound is obtained

Vorschrift

This compound is obtained according to the procedure described in 1.2. by reacting unpurified 3,5-dimethoxy-2-(phenylacetyl)benzoic acid with hydrazine hydrate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423030B2uspto-grants-2008_09