Reaktion #58237

ord-904c656ff4f64bd5a69094fa4732ab91

Reaktionsgleichung

COc1ccc(Br)c(C(=O)O)c1
2-bromo-5-methoxybenzoic acid
[Li][CH2]CCC
n-butyllithium
CCC(=O)N(C)OC
N-methoxy-N-methylpropionamide
CCC(=O)c1ccc(OC)cc1C(=O)O
5-methoxy-2-propionylbenzoic acid

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThis compound is synthesized
  2. 2
    Sonstigein the following reaction

Vorschrift

This compound is synthesized according to the method described in 3.2. by reacting 2-bromo-5-methoxybenzoic acid pretreated with n-butyllithium with N-methoxy-N-methylpropionamide. It is used in crude form in the following reaction.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423030B2uspto-grants-2008_09