Reaktion #58187

ord-35fabb36465e486b9c0aec2d61cb78bb

Reaktionsgleichung

O=[N+]([O-])c1cccc(-c2nc(O)c3c(n2)CCN(Cc2ccccc2)C3)c1
6-benzyl-2-(3-nitro-phenyl)-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol
O=[N+]([O-])c1cccc(-c2nc(O)c3c(n2)CCN(Cc2ccccc2)C3)c1
Intermediate 9
O=[N+]([O-])c1cccc(-c2nc(O)c3c(n2)CCN(Cc2ccccc2)C3)c1
6-benzyl-2-(3-nitro-phenyl)-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol
N#Cc1ccc(CBr)cc1
4-cyanobenzyl bromide
N#Cc1ccc(COc2nc(-c3cccc([N+](=O)[O-])c3)nc3c2CN(Cc2ccccc2)CC3)cc1
title compound
N#Cc1ccc(COc2nc(-c3cccc([N+](=O)[O-])c3)nc3c2CN(Cc2ccccc2)CC3)cc1
4-({[6-Benzyl-2-(3-nitrophenyl)-5,6,7,8-tetrahydropyrido[4,3-d]pyrimidin-4-yl]oxy}methyl)benzonitrile

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 6-benzyl-2-(3-nitro-phenyl)-5,6,7,8-tetrahydro-pyrido[4,3-d]pyrimidin-4-ol (which was obtained in Intermediate 9) and 4-cyanobenzyl bromide according to Method A; LC retention time 2.53 min; MS: m/z (ESI) 478 (M+H).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423044B2uspto-grants-2008_09