Reaktion #58184

ord-52bde15521394de9bf08913cd8331e89

Reaktionsgleichung

CC(C)c1cc(O)nc(-c2cc(Cl)cc(Cl)c2)n1
2-(3,5-dichloro-phenyl)-6-isopropyl-pyrimidin-4-ol
CC(C)c1cc(O)nc(-c2cc(Cl)cc(Cl)c2)n1
Intermediate 6
CC(C)c1cc(O)nc(-c2cc(Cl)cc(Cl)c2)n1
2-(3,5-dichloro-phenyl)-6-isopropyl-pyrimidin-4-ol
N#Cc1ccc(CBr)cc1
4-cyanobenzyl bromide
CC(C)c1cc(OCc2ccc(C#N)cc2)nc(-c2cc(Cl)cc(Cl)c2)n1
title compound
CC(C)c1cc(OCc2ccc(C#N)cc2)nc(-c2cc(Cl)cc(Cl)c2)n1
4-({[2-(3,5-Dichlorophenyl)-6-isopropylpyrimidin-4-yl]oxy}methyl)benzonitrile

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared from 2-(3,5-dichloro-phenyl)-6-isopropyl-pyrimidin-4-ol (which was obtained in Intermediate 6) and 4-cyanobenzyl bromide according to Method A; LC retention time 4.22 min; MS: m/z (ESI) 398 (M+H).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07423044B2uspto-grants-2008_09