Reaktion #58008

Reaktionsgleichung

para-fluoronitrobenzene

m-xylenediamine

triethylamine

→

4-nitro-N-(3-{[(4-nitrophenyl)amino]methyl}benzyl)aniline

Lösungsmittel

DMSO

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONThe mixture was then poured
2. 2
   Sonstigeonto crushed ice
3. 3
   Sonstigea precipitate formed
4. 4
   FiltrationThe latter was filtered
5. 5
   Waschenwashed with water
6. 6
   Sonstigedried

Vorschrift

1.73 g of para-fluoronitrobenzene (2 eq.) were dissolved in 5 ml of DMSO. 1.2 equivalents of m-xylenediamine and 4 equivalents of triethylamine were added to the solution. The reaction mixture was heated at 60° C. for 20 hours. The mixture was then poured onto crushed ice and a precipitate formed. The latter was filtered, washed with water, and then dried.

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