Reaktion #575657

ord-dd23df0b12d34f938cdba6f0864d81b7

Reaktionsgleichung

CCOC(=O)c1c(C)nc(Br)n1C
2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester
C#Cc1ccc(N)cc1
4-ethynylaniline
CCOC(=O)c1c(C)nc(C#Cc2ccc(N)cc2)n1C
title compound
CCOC(=O)c1c(C)nc(C#Cc2ccc(N)cc2)n1C
2-(4-Amino-phenylethynyl)-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound, MS: m/e=284.4 (M+H+) was prepared in accordance with the general method of example 1b from 2-bromo-3,5-dimethyl-3H-imidazole-4-carboxylic acid ethyl ester and 4-ethynylaniline.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06972299B2uspto-grants-2005_12