Reaktion #575494

ord-07762ec257ee4d0faf242acdda9d0ae5

Reaktionsgleichung

COC(=O)c1cc(O)ccc1O
2,5-dihydroxybenzoic acid methyl ester
CCCCCCCCCCBr
1-bromodecane
CCCCCCCCCCOc1ccc(O)c(C(=O)OC)c1
5-(decyloxy)-2-hydroxybenzoic acid methyl ester
Ausbeute 51.0%

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The reaction of 2,5-dihydroxybenzoic acid methyl ester with 1-bromodecane under conditions described in Example 58 gave 5-(decyloxy)-2-hydroxybenzoic acid methyl ester (51% yield, mp 40°-43°).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05298652uspto-grants-1994_03