Reaktion #56961

ord-26e60dcdcac143cd8beddff7c5a46472

Reaktionsgleichung

NC1CCCc2c1[nH]c1ccc(Br)cc21
6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine
O=C(Cl)C=Cc1ccccc1
cinnamoyl chloride
→
O=C(C=Cc1ccccc1)NC1CCCc2c1[nH]c1ccc(Br)cc21
N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-3-phenylprop-2-enamide

Edukte

NC1CCCc2c1[nH]c1ccc(Br)cc21
6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine
O=C(Cl)C=Cc1ccccc1
cinnamoyl chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

N-(6-Bromo-2,3,4,9-tetrahydro-1H-carbazol-1-yl)-3-phenylprop-2-enamide was prepared from 6-bromo-2,3,4,9-tetrahydro-1H-carbazol-1-amine and cinnamoyl chloride in a similar manner as described above to give an off-white solid (35% yield).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07419997B2uspto-grants-2008_09