Reaktion #56829

Reaktionsgleichung

5-chloro-2-methoxy-benzimidic acid ethyl ester

ammonia

→

5-chloro-2-methoxy-benzylideneamine

Ausbeute 129.0%

Lösungsmittel

methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeEvaporation of volatiles under reduced pressure

Vorschrift

A mixture of 5-chloro-2-methoxy-benzimidic acid ethyl ester (1.0 g, 4.0 mmol) and a solution of ammonia in methanol (7.0 M, 50 ml) was stirred for 48 hours. Evaporation of volatiles under reduced pressure provided 5-chloro-2-methoxy-benzylideneamine (0.875 g, 99% yield).

Quelle