Reaktion #566697

ord-2fb87f3f0e114916aaa93dcaec2c0921

Reaktionsgleichung

Cc1ccc(S(=O)(=O)O)cc1
p-toluenesulfonic acid
c1ccc2[nH]nnc2c1
Benzotriazole
NC(=O)c1ccc(Cl)cc1
4-chlorobenzamide
C=CCC(C)(C)C=O
2,2-dimethyl-4-pentenal
→
C=CCC(C)(C)C(NC(=O)c1ccc(Cl)cc1)n1nnc2ccccc21
N-[1-(1H-1,2,3-benzotriazol-1-yl)-2,2-dimethyl-4-pentenyl]-4-chlorobenzamide

Edukte

Cc1ccc(S(=O)(=O)O)cc1
p-toluenesulfonic acid
c1ccc2[nH]nnc2c1
Benzotriazole
NC(=O)c1ccc(Cl)cc1
4-chlorobenzamide
C=CCC(C)(C)C=O
2,2-dimethyl-4-pentenal

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigeto provide Example 67A

Vorschrift

Benzotriazole, 4-chlorobenzamide, 2,2-dimethyl-4-pentenal, and p-toluenesulfonic acid were processed as in Example 53A to provide Example 67A.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06645968B2uspto-grants-2003_11