Reaktion #56521

Reaktionsgleichung

isoamyl nitrite

benzene

2,4-difluoroaniline

→

2,4-difluorobiphenyl

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturthermometer, nitrogen-inlet, internal steam coil and reflux condenser

Vorschrift

To a 50 liter resin pot equipped with stirrer, thermometer, nitrogen-inlet, internal steam coil and reflux condenser is charged 31.5 liters of benzene, 1.025 liters of isoamyl nitrite and 700 g. (5.43 moles) of 2,4-difluoroaniline.

Quelle