Reaktion #56491

Reaktionsgleichung

methanol

ethyl 2-chloro-4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate

ethyl 4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate

→

title compound

Ethyl 2-Chloro-4-{3-[3-[2-(1-Cyclohexenyl)ethyl]-4-oxo-2-thiazolidinyl]propyl}benzoate

Lösungsmittel

chloroform

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThis compound is prepared by the method

Vorschrift

This compound is prepared by the method described in Example 4, Step B, except that an equivalent quantity of ethyl 2-chloro-4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate is substituted for the ethyl 4-[3-(4-oxo-2-thiazolidinyl)propyl]benzoate of Example 4, Step B. The title compound is obtained as an oil by column chromatography on silica gel with 2% methanol in chloroform as eluant.

Quelle