Reaktion #5636

ord-9589a48d34f74be29e906b317fd0389c

Reaktionsgleichung

Nc1ccc(N)cc1
p-phenylenediamine
Nc1ccc(-c2ccc(N)cc2)cc1
benzidine
→
Nc1ccc(N(c2ccc(N)cc2)c2ccc(-c3ccc(N(c4ccc(N)cc4)c4ccc(N)cc4)cc3)cc2)cc1
tetrakis (p-aminophenyl)benzidine

Edukte

Nc1ccc(N)cc1
p-phenylenediamine
Nc1ccc(-c2ccc(N)cc2)cc1
benzidine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe same reaction
  2. 2
    Sonstigeas in Synthesis example 1

Vorschrift

The same reaction as in Synthesis example 1 was carried out except for changing p-phenylenediamine used in Synthesis example 1 to benzidine to obtain 12 parts of orange tetrakis (p-aminophenyl)benzidine.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05245030uspto-grants-1993_09