Reaktion #56258

ord-310402dfa2b2420b82f5826c743adfae

Reaktionsgleichung

CN(C)CCN
dimethylaminoethylamine
CN(C)CCNC(=O)C(O)[C@H]1O[C@@H](n2cnc3c(N)ncnc32)[C@H](O)[C@@H]1O
adenosine-5'-carboxylic acid N-(2-dimethylaminoethyl)-amide
→
C=CCNC(=O)C(O)[C@H]1O[C@@H](n2cnc3c(N)ncnc32)[C@H](O)[C@@H]1O
Adenosine-5'-carboxylic acid N-allylamide
Ausbeute 84.0%

Edukte

CN(C)CCN
dimethylaminoethylamine
CN(C)CCNC(=O)C(O)[C@H]1O[C@@H](n2cnc3c(N)ncnc32)[C@H](O)[C@@H]1O
adenosine-5'-carboxylic acid N-(2-dimethylaminoethyl)-amide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

with dimethylaminoethylamine: adenosine-5'-carboxylic acid N-(2-dimethylaminoethyl)-amide; m.p. 136°-138° C.; yield 84% of theory.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04224438uspto-grants-1980_09