Reaktion #56196

Reaktionsgleichung

p-Chlorophenylhydroxylamine

ethanol

p-cyclohexylbenzaldehyde

→

α-p-cyclohexylphenyl-N-p-chlorophenylnitrone

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solid which formed
2. 2
   Sonstigewas collected
3. 3
   Waschenwashed with 95% ethanol
4. 4
   Sonstigewas recrystallized from ethanol

Vorschrift

p-Chlorophenylhydroxylamine (0.05 moles) was dissolved in warm 95% ethanol (40 cc) and was treated with p-cyclohexylbenzaldehyde (0.05 moles) with vigorous stirring. The solid which formed was collected, washed with 95% ethanol, and was recrystallized from ethanol to give α-p-cyclohexylphenyl-N-p-chlorophenylnitrone.

Quelle