Reaktion #56163

Reaktionsgleichung

1,8-Diaminonaphthalene

p-Trifluoromethoxybenzoyl fluoride

→

2-(p-TRIFLUOROMETHOXYPHENYL)-1H-PERIMIDINE HYDROFLUORIDE

Lösungsmittel

toluene

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigeof toluene, then decanted
2. 2
   workup.ADDITIONBoth solutions were added simultaneously to 25 ml

Vorschrift

1,8-Diaminonaphthalene (1.52 grams; 0.0096 mole) was dissolved in 25 ml. of toluene, then decanted. p-Trifluoromethoxybenzoyl fluoride (2.0 grams; 0.0096 mole) was dissolved in 25 ml. of toluene. Both solutions were added simultaneously to 25 ml. of toluene. After the reaction mixture had been stirred for approximately 4 hours, TLC indicated that the reaction was complete.

Quelle