Reaktion #56152

ord-2dc269c23b514a9789547f511597a9fb

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
130°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONthere are slowly added

Vorschrift

To 32 g (0.1 mole) of isostearic acid there is added 0.3 ml (0.002 mole) of triethylamine. The resulting mixture is heated to 130° C. under a nitrogen atmosphere and there are slowly added thereto 40 g (0.1 mole) of 2-octyl dodecyl ether of glycidyl obtained according to the above method. After heating for 3 hours and 15 minutes at 130° C., the amount of the reaction determined by acid index is 93%.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04224311uspto-grants-1980_09