Reaktion #56112

ord-b4024651ddb646fda3b64ce73c2962c6

Reaktionsgleichung

C=C(C)C(=O)OCCN(C)C
DMAEMA
C=CC(N)=O
acrylamide
C=C(C)C(=O)OCCN(C)C
DMAEMA
→
C=C(C)C(=O)OCCN(C)C.C=CC(N)=O
Acrylamide DMAEMA

Edukte

C=C(C)C(=O)OCCN(C)C
DMAEMA
C=CC(N)=O
acrylamide
C=C(C)C(=O)OCCN(C)C
DMAEMA

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
85°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigethe effect of reaction temperature on the quat content
  2. 2
    workup.ADDITIONwas added

Vorschrift

This example demonstrates the effect of reaction temperature on the quat content. Example 9C was repeated except that the temperature was raised to 85° C. before the initiator was added. After 6 hours G.L.C. analysis showed no DMAEMA and no acrylamide present. This indicates that none of the DMAEMA had been quaternized.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04224150uspto-grants-1980_09