Reaktion #558896

ord-cfe14242c0ca4caabd146131bdf52d9a

Reaktionsgleichung

CC(C)(O)CCO
3-methylbutane-1,3-diol
N#Cc1c([N+](=O)[O-])cccc1[N+](=O)[O-]
2,6-dinitrobenzonitrile
→
CC(C)(O)CCOc1cccc([N+](=O)[O-])c1C#N
2-(3-hydroxy-3-methylbutoxy)-6-nitrobenzonitrile
Ausbeute 81.0%

Edukte

CC(C)(O)CCO
3-methylbutane-1,3-diol
N#Cc1c([N+](=O)[O-])cccc1[N+](=O)[O-]
2,6-dinitrobenzonitrile

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared as in Example 215c from 3-methylbutane-1,3-diol and 2,6-dinitrobenzonitrile in 81% yield. MS 251 (MH+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08633186B2uspto-grants-2014_01