Reaktion #558884

ord-18a8f9534a724127976a3d58ca293403

Reaktionsgleichung

CCNC(=O)NCC(C)(C)CO
1-ethyl-3-(3-hydroxy-2,2-dimethylpropyl)urea
N#Cc1c([N+](=O)[O-])cccc1[N+](=O)[O-]
2,6-dinitrobenzonitrile
→
CCNC(=O)NCC(C)(C)COc1cccc([N+](=O)[O-])c1C#N
1-(3-(2-cyano-3-nitrophenoxy)-2,2-dimethylpropyl)-3-ethylurea
Ausbeute 47.0%

Edukte

CCNC(=O)NCC(C)(C)CO
1-ethyl-3-(3-hydroxy-2,2-dimethylpropyl)urea
N#Cc1c([N+](=O)[O-])cccc1[N+](=O)[O-]
2,6-dinitrobenzonitrile

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared as in Example 215c from 1-ethyl-3-(3-hydroxy-2,2-dimethylpropyl)urea (Example 227d) and 2,6-dinitrobenzonitrile in 47% yield. MS 321 (MH+).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08633186B2uspto-grants-2014_01