Reaktion #55807

ord-bad7e6a3ee4b40c5b663da29be26ce89

Reaktionsgleichung

NCCNCc1cccnn1
N-(3-pyridazinylmethyl)ethylenediamine
CSC(=N)N[N+](=O)[O-]
S-methyl-N-nitroisothiourea
→
N=C(NCCNCc1cccnn1)N[N+](=O)[O-]
N-nitro-N'-[2-(3-pyridazinylmethylamino)ethyl]guanidine

Edukte

NCCNCc1cccnn1
N-(3-pyridazinylmethyl)ethylenediamine
CSC(=N)N[N+](=O)[O-]
S-methyl-N-nitroisothiourea

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Reacting N-(3-pyridazinylmethyl)ethylenediamine with S-methyl-N-nitroisothiourea by the procedure of Example 2(ii) give N-nitro-N'-[2-(3-pyridazinylmethylamino)ethyl]guanidine. Treatment with hydrobromic acid gives the hydrobromide salt.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04221802uspto-grants-1980_09