Reaktion #55656

ord-84ea0d37cd7e4ceea09e7d996fe0f21e

Reaktionsgleichung

O=C(c1ccccc1)c1ccc(Cl)c([N+](=O)[O-])c1
3-nitro-4-chloro-benzophenone
CCNC1CCCCC1
N-ethyl-N-cyclohexylamine
→
CCN(c1ccc(C(=O)c2ccccc2)cc1[N+](=O)[O-])C1CCCCC1
3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone

Edukte

O=C(c1ccccc1)c1ccc(Cl)c([N+](=O)[O-])c1
3-nitro-4-chloro-benzophenone
CCNC1CCCCC1
N-ethyl-N-cyclohexylamine

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe crude product is recrystallized from n-hexane

Vorschrift

13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04221739uspto-grants-1980_09