Reaktion #55590

Reaktionsgleichung

p-toluenesulfonic acid monohydrate

acetone

→

title compound

8-oxononan-1-ol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe acetone was removed in vacuo

Vorschrift

A solution containing 56.6 g of 8-oxononan-1-ol ethylene ketol (prepared in Example 22 B-5) in 210 ml acetone and 50 mg p-toluenesulfonic acid monohydrate was stirred at room temperature for about 15 to 17 hr. The acetone was removed in vacuo to yield the title compound having the following physical characteristics:

Quelle