Reaktion #55575

ord-50d29d0bae2248dc857e5a27e9aae21e

Reaktionsgleichung

CCCCI
1-iodobutane
CCC1CC(C(=O)O)C1
3-ethylcyclobutanecarboxylic acid
CI
methyl iodide
O=C(O)C1CCC1
cyclobutanecarboxylic acid
→
CCCCC1(C(=O)O)CCC1
title compound
CCCCC1(C(=O)O)CCC1
1-Butylcyclobutanecarboxylic acid

Edukte

CCCCI
1-iodobutane
CCC1CC(C(=O)O)C1
3-ethylcyclobutanecarboxylic acid
CI
methyl iodide
—
resultant product
O=C(O)C1CCC1
cyclobutanecarboxylic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared as in Example 2A by replacing 3-ethylcyclobutanecarboxylic acid and methyl iodide respectively with cyclobutanecarboxylic acid and 1-iodobutane (Aldrich Chemical Company; Beilstein 1: 123). The resultant product had the following physical characterisics:

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04220795uspto-grants-1980_09