Reaktion #55417

Reaktionsgleichung

11-aminoundecanoic acid

methyl carboxydithiocarbamate

sodium azide

7-aminoheptanoic acid

9-aminononanoic acid

→

1-(6-carboxyhexyl)tetrazole-5-thiol

1-(8-carboxyoctyl)tetrazole-5-thiol

Reaktionsbedingungen

Vorschrift

When 7-aminoheptanoic acid or 9-aminononanoic acid is substituted in the procedure of Example 19 in place of 11-aminoundecanoic acid and the resulting methyl carboxydithiocarbamate is treated with sodium azide as described therein, 1-(6-carboxyhexyl)tetrazole-5-thiol and 1-(8-carboxyoctyl)tetrazole-5-thiol are obtained, respectively.

Quelle