Reaktion #55386

Reaktionsgleichung

3-mercapto-1,2,4-triazole

3-aminopropanol

hydrobromic acid

→

3-(3-aminopropylthio)-1,2,4-triazole dihydrobromide

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturunder reflux for 24 hours
2. 2
   SonstigeThe reaction mixture is evaporated to dryness
3. 3
   Sonstigethe residue recrystallised from ethanol/ether

Vorschrift

A solution of 3-mercapto-1,2,4-triazole and 3-aminopropanol in hydrobromic acid is heated under reflux for 24 hours. The reaction mixture is evaporated to dryness and the residue recrystallised from ethanol/ether to give 3-(3-aminopropylthio)-1,2,4-triazole dihydrobromide.

Quelle