Reaktion #55128

ord-2e29091de0cd4d22a353d94107be094b

Reaktionsgleichung

NCCSCc1cccnn1
3-[(2-aminoethyl)-thiomethyl]pyridazine
O=C(N=C=S)c1ccccc1
benzoyl isothiocyanate
O=C(NC(=S)NCCSCc1cccnn1)c1ccccc1
N-benzoyl-N'-[2-(3-pyridazinylmethylthio)ethyl]thiourea

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

By the procedure of Example 18, 3-[(2-aminoethyl)-thiomethyl]pyridazine is reacted with benzoyl isothiocyanate to give N-benzoyl-N'-[2-(3-pyridazinylmethylthio)ethyl]thiourea. Removing the benzoyl group by the procedure of Example 18 gives N-[2-(3-pyridazinylmethylthio)ethyl]thiourea.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04151288uspto-grants-1979_04