Reaktion #55110

ord-88f83fb8b4c04d4d87fa24d8155d1664

Reaktionsgleichung

NCCSCc1cc[nH]n1
3-[(2-aminoethyl)-thiomethyl]pyrazole
O=C(N=C=S)c1ccccc1
benzoyl isothiocyanate
O=C(NC(=S)NCCSCc1cc[nH]n1)c1ccccc1
N-benzoyl-N'-[2-(3-pyrazolylmethylthio)ethyl]thiourea

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

By the procedure of Example 18, 3-[(2-aminoethyl)-thiomethyl]pyrazole is reacted with benzoyl isothiocyanate to give N-benzoyl-N'-[2-(3-pyrazolylmethylthio)ethyl]thiourea. Removing the benzoyl group by the procedure of Example 18 gives N-[2-(3-pyrazolylmethylthio)ethyl]thiourea.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04151288uspto-grants-1979_04