Reaktion #550578
ord-fedc18279f2c41e39a7646f546a1f17a
Reaktionsgleichung
Ethyl 2-methoxyimino-3,3-diethoxybutyrate
pyridinium hydrobromide
→
ethyl 2-methoxyimino-3,3-diethoxy-4-bromobutyrate
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
Ethyl 2-methoxyimino-3,3-diethoxybutyrate (syn isomer, 10.0 g), pyridinium hydrobromide perbromide (15.5 g) and tetrahydrofuran (100 ml) were treated in a similar manner to that of Example 8 (2) to give ethyl 2-methoxyimino-3,3-diethoxy-4-bromobutyrate (syn isomer, 16.20 g).