Reaktion #550393

ord-c94b7a47f73046509116cd1f72e1632d

Reaktionsgleichung

CCC1(CC)OC(=O)Nc2ccc(OCCCCSc3ccc(OC)c(OC)c3)cc21
6-[4-(3,4-dimethoxy-phenylmercapto)-butoxy]-4,4-diethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide
→
CCC1(CC)OC(=O)Nc2ccc(OCCCCS(=O)c3ccc(OC)c(OC)c3)cc21
6-[4-(3,4-Dimethoxy-phenylsulfinyl)-butoxy]-4,4-diethyl-4H-3,1-benzoxazin-2-one

Edukte

CCC1(CC)OC(=O)Nc2ccc(OCCCCSc3ccc(OC)c(OC)c3)cc21
6-[4-(3,4-dimethoxy-phenylmercapto)-butoxy]-4,4-diethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared analogously to Example 2 from 6-[4-(3,4-dimethoxy-phenylmercapto)-butoxy]-4,4-diethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04518597uspto-grants-1985_05