Reaktion #550382

ord-ce3ccb81999c4bb9823421e35c3b6d63

Reaktionsgleichung

CC(=O)Nc1ccc(SCCCCOc2ccc3c(c2)NC(=O)OC3(C)C)cc1
7-[4-(4-acetamido-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide
→
CC(=O)Nc1ccc(S(=O)CCCCOc2ccc3c(c2)NC(=O)OC3(C)C)cc1
7-[4-(4-Acetamido-phenylsulfinyl)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Edukte

CC(=O)Nc1ccc(SCCCCOc2ccc3c(c2)NC(=O)OC3(C)C)cc1
7-[4-(4-acetamido-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared analogously to Example 2 from 7-[4-(4-acetamido-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04518597uspto-grants-1985_05