Reaktion #550303

ord-d4e4685162a94bb8ba135ca4d755d434

Reaktionsgleichung

COc1ccc(SCCCCOc2ccc3c(c2)C(C)(C)OC(=O)N3)cc1
6-[4-(4-methoxy-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide
→
COc1ccc(S(=O)CCCCOc2ccc3c(c2)C(C)(C)OC(=O)N3)cc1
6-[4-(4-Methoxy-phenylsulfinyl)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Edukte

COc1ccc(SCCCCOc2ccc3c(c2)C(C)(C)OC(=O)N3)cc1
6-[4-(4-methoxy-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared analogously to Example 2 from 6-[4-(4-methoxy-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04518597uspto-grants-1985_05