Reaktion #550301

ord-8a8b09a5fa3f4867ad9f64ef0a44988e

Reaktionsgleichung

CC1(C)OC(=O)Nc2ccc(OCCCCSc3ccc(F)cc3)cc21
6-[4-(4-fluoro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide
→
CC1(C)OC(=O)Nc2ccc(OCCCCS(=O)c3ccc(F)cc3)cc21
6-[4-(4-Fluoro-phenylsulfinyl)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one

Edukte

CC1(C)OC(=O)Nc2ccc(OCCCCSc3ccc(F)cc3)cc21
6-[4-(4-fluoro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one
OO
hydrogen peroxide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Prepared analogously to Example 2 from 6-[4-(4-fluoro-phenylmercapto)-butoxy]-4,4-dimethyl-4H-3,1-benzoxazin-2-one and hydrogen peroxide.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04518597uspto-grants-1985_05