Reaktion #54984

Reaktionsgleichung

ethoxyacetyl chloride

N-(1'-methyl-2'-methoxyethyl)-2,6-dimethylaniline

→

N-(1'-methyl-2'-methoxyethyl)-N-ethoxyacetyl-2,6-dimethylaniline

Lösungsmittel

toluene

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.STIRRINGAfter stirring for 3 hours at room temperature
2. 2
   Filtrationthe reaction mixture was filtered
3. 3
   workup.DISTILLATIONthe residual oil was distilled in a high vacuum

Vorschrift

With stirring, 7.3 g of ethoxyacetyl chloride in 20 ml of abs. toluene were added at room temperature to 9.6 g of N-(1'-methyl-2'-methoxyethyl)-2,6-dimethylaniline. After stirring for 3 hours at room temperature, the reaction mixture was filtered. The filtrate was freed from solvent and the residual oil was distilled in a high vacuum. Boiling point: 122°-124° C./0.04 torr.

Quelle