Reaktion #54975

ord-74b6859fd148429f92bec5fdefd4dd3d

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

0.10 mole resorcinol and 0.12 mole sodium diethyl oxalacetate is heated to 80° C. for 1 hour in 60 ml concentrated phosphoric acid. 4-Carbethoxy-7-hydroxy-coumarin is thus obtained at an 80% yield in the form of a viscous oil.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04151291uspto-grants-1979_04