Reaktion #54949

Reaktionsgleichung

anisole

3-acetylaminophenol

→

2-hydroxy-4-acetylaminobenzaldehyde

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigea temperature of 100° C.
2. 2
   Sonstigeyield on the theoretical value=50%)
3. 3
   Sonstigeat 185°-186° C.
4. 4
   Sonstigewere obtained

Vorschrift

By operating according to Example 13, but using anisole as the solvent and a temperature of 100° C., and starting from 15.1 g of 3-acetylaminophenol, 9.0 g of a product (yield on the theoretical value=50%) having a melting point at 185°-186° C. were obtained.

Quelle