Reaktion #54827

Reaktionsgleichung

ethyl 3-amino-4-cyclohexylphenylglyoxylate

methyl iodide

→

ethyl 3-methylamino-4-cyclohexylphenylglyoxylate

Lösungsmittel

pyridine

Reaktionsbedingungen

Aufarbeitung

1. 1
   Filtrationfiltered
2. 2
   Einengenconcentrated
3. 3
   workup.DISTILLATIONThe residue is distilled

Vorschrift

To a solution of 0.01 moles of ethyl 3-amino-4-cyclohexylphenylglyoxylate in 100 ml. of pyridine is added 0.1 moles of methyl iodide. The reaction mixture is stirred overnight at room temperature, filtered and concentrated. The residue is distilled to obtain ethyl 3-methylamino-4-cyclohexylphenylglyoxylate.

Quelle