Reaktion #547690

ord-83770ba9fa59423daa05a4705525ebfc

Reaktionsgleichung

O=[N+]([O-])c1ccc(O)cc1Nc1ccccc1
3-phenylamino-4-nitrophenol
COC(=O)CCCCCBr
6-bromohexanoic acid methyl ester
→
COC(=O)CCCCCOc1ccc([N+](=O)[O-])c(Nc2ccccc2)c1
6-(3-Phenylamino-4-nitrophenyl)oxyhexanoic acid methyl ester

Edukte

O=[N+]([O-])c1ccc(O)cc1Nc1ccccc1
3-phenylamino-4-nitrophenol
COC(=O)CCCCCBr
6-bromohexanoic acid methyl ester

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstige11.2 g was obtained

Vorschrift

13.3 g of 3-phenylamino-4-nitrophenol was reacted with 6-bromohexanoic acid methyl ester according to general operating instructions 2. 11.2 g was obtained.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07196202B2uspto-grants-2007_03