Reaktion #54765

ord-25733b55cc1b4cf7b7f098dddb0f0373

Reaktionsgleichung

O=C(CO)c1ccccc1
phenacyl alcohol
CCCCNC#N
butylcyanamide
→
CCCCNc1nc(-c2ccccc2)co1
2-(N-Butylamino)-4-phenyloxazole

Edukte

O=C(CO)c1ccccc1
phenacyl alcohol
CCCCNC#N
butylcyanamide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeA colourless oil was obtained
  2. 2
    workup.DISTILLATIONafter distillation of the product

Vorschrift

The procedure as described in Example 1 was followed using phenacyl alcohol and butylcyanamide. A colourless oil was obtained after distillation of the product.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04150143uspto-grants-1979_04