Reaktion #547306

Reaktionsgleichung

2-amino-4-bromophenol

trimethyl orthoacetate

→

title compound

2-methyl-5-bromobenzoxazole

Reaktionsbedingungen

Aufarbeitung

1. 1
   TemperaturThe reaction was then cooled
2. 2
   Sonstigethe solvent removed under reduced pressure

Vorschrift

A solution of 2-amino-4-bromophenol (1 g, 5.32 mmol) in trimethyl orthoacetate (20 mL) was refluxed for 1.5 hours. The reaction was then cooled and the solvent removed under reduced pressure to give 1.1 g of title compound.

Quelle