Reaktion #54666

Reaktionsgleichung

p-menth-3-oyl chloride

glycine propyl ester hydrochloride

sodium bicarbonate

→

N-p-Menth-3-oylglycine n-propyl ester

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.DISTILLATIONThe crude product was distilled b.p. 170°/0.1 mm
2. 2
   workup.DISTILLATION(After distillation the product

Vorschrift

Following the procedure of Example 2 p-menth-3-oyl chloride (2.0 g., 0.01 moles), was reacted with glycine propyl ester hydrochloride (1.5 g., 0.01 moles) and sodium bicarbonate (1.6 g., 0.02 moles). The crude product was distilled b.p. 170°/0.1 mm. (After distillation the product rapidly solidifies). (Found, C: 68.2; H: 1016; N: 5.0. C16H29NO3 requires, C: 67.8; H: 10.6; N: 4.9.)

Quelle