Reaktion #54540

ord-ca4477f096bc46d990edfe697841cf74

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    TemperaturThe solution is further refluxed for 30 minutes
  2. 2
    Sonstigeis then evaporated to dryness

Vorschrift

To a boiling aqueous solution of sodium bisulfite (1.47 g, 0.0141 mole) is added in portions p-chloromethylphenylacetic acid (2.6 g, 0.0141 mole). The solution is further refluxed for 30 minutes and is then evaporated to dryness to give a quantitative yield of the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04148997uspto-grants-1979_04