Reaktion #54210

ord-467d9d755ab0419eb229071237b703c5

Reaktionsgleichung

C=Cc1ccccc1
Styrene
C=Cc1ccncc1
4-vinylpyridine
C=Cc1ccccc1C=C
divinylbenzene
CC(C)(C#N)N=NC(C)(C)C#N
azobisisobutyronitrile
→
C=Cc1ccccc1.C=Cc1ccccc1C=C.C=Cc1ccncc1
fine white solids
C=Cc1ccccc1.C=Cc1ccccc1C=C.C=Cc1ccncc1
4-Vinylpyridine styrene-divinylbenzene

Edukte

C=Cc1ccccc1
Styrene
C=Cc1ccncc1
4-vinylpyridine
C=Cc1ccccc1C=C
divinylbenzene
CC(C)(C#N)N=NC(C)(C)C#N
azobisisobutyronitrile

Reagenzien

Keine

Lösungsmittel

O
water

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Styrene (73 grams), 4-vinylpyridine (24 grams), 600 ml of water, divinylbenzene (4 grams), Natrasol 250H and azobisisobutyronitrile reacted as in Example 1. Obtained 88 grams of fine white solids, 3.3% nitrogen.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04147730uspto-grants-1979_04