Reaktion #54209

ord-160d52d13306401890cc3c52431d6e5b

Reaktionsgleichung

O=[N+]([O-])c1ccccc1
Nitrobenzene
CC(C)=O
acetone
→
CC(=O)c1ccc(-c2cccc(-c3ccccc3)c2)cc1
crude product
CC(=O)c1ccc(-c2cccc(-c3ccccc3)c2)cc1
4-acetyl m-terphenyl

Edukte

O=[N+]([O-])c1ccccc1
Nitrobenzene
CC(C)=O
acetone

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    FiltrationAfter filtration
  2. 2
    Sonstigethe acetone evaporation

Vorschrift

Nitrobenzene is stripped with steam and the solid residue is dissolved into acetone. After filtration and the acetone evaporation, 400 g of crude product is obtained.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04147728uspto-grants-1979_04