Reaktion #5397

ord-38a46896cfd64460abeefed1d758aed6

Reaktionsgleichung

OCc1ccccc1
benzyl alcohol
CO
methanol
O=C1OCc2ccccc21
phthalide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The procedure described in method F is repeated, except that the methanol is replaced by 50 ml of benzyl alcohol, affording a phthalide compound of the formula ##STR19## melting point 183°-184° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05244860uspto-grants-1993_09