Reaktion #53793

Reaktionsgleichung

product

5-(1H-Indol-2-yl)-2-methoxy-phenylamine

5-(1H-indol-2-yl)-2-methoxy-phenylamine

thiophosgene

→

[5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate

Reaktionsbedingungen

Vorschrift

The product from Example 1, 5-(1H-indol-2-yl)-2-methoxy-phenylamine, (4.76 g, 20 mmol) was reacted with thiophosgene (1.9 mL, 25 mmol) according to the procedure for Example 23, Step A, to give [5-(1H-indol-2-yl)-2-methoxy-phenyl]-isothiocyanate (4.55 g), as a black solid.

Quelle